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CSN-010 Epoxy Resin

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    Specifications
    HS Code 615522
    Productname CSN-010 Epoxy Resin
    Producttype Two-component room-temperature-cure epoxy resin
    Appearance Clear, transparent liquid
    Mixratiobyweight 2:1 (A:B)
    Mixratiobyvolume 2:1 (A:B)
    Viscosityat25c 2500-3500 mPa·s
    Densityat25c 1.10-1.15 g/cm³
    Potlifeat25c 30-40 min for 100 g mix
    Curetimeat25c 24 h
    Curetimeat60c 2 h
    Shoredhardness 80-85
    Tensilestrength 45-55 MPa
    Flexuralstrength 80-100 MPa
    Compressivestrength 80-95 MPa
    Glasstransitiontemperature 60-70 °C
    Operatingtemperaturerange -40 to 100 °C
    Waterabsorption <0.2%
    Dielectricstrength 15-20 kV/mm
    Shelflife 12 months
    Storagetemperature 15-25 °C

    As an accredited CSN-010 Epoxy Resin factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing CSN-010 Epoxy Resin is supplied in sealed 5 kg plastic pails, clearly labeled with hazard and handling information.
    Container Loading (20′ FCL) CSN-010 Epoxy Resin loaded into a 20-foot FCL container, palletized, properly secured, and sealed for safe ocean shipment.
    Shipping CSN-010 Epoxy Resin should be shipped in sealed, labeled containers with secondary containment, protected from moisture, heat, and freezing. Keep in a cool, dry, ventilated area. Consult the SDS and applicable transport regulations for UN classification, packaging, labeling, and any hazardous-goods requirements before shipment.
    Storage Store CSN-010 Epoxy Resin in a cool, dry, well-ventilated area away from heat, sparks, flames, and direct sunlight. Keep containers tightly closed when not in use to prevent moisture contamination. Store separately from incompatible chemicals such as strong acids, bases, and oxidizers. Use secondary containment where appropriate, and follow the manufacturer’s SDS and local regulations.
    Shelf Life CSN-010 Epoxy Resin shelf life is typically 12–24 months when stored unopened, cool, dry, and protected from light and moisture.
    Application of CSN-010 Epoxy Resin

    In filament winding of Type IV composite pressure vessels, CSN-010 is specified as the base resin for amine-cured hoop and helical layers. The resin is batched at 100 phr with methyltetrahydrophthalic anhydride at 85 phr and 1,2-dimethylimidazole at 0.6 phr. Vacuum degassing at −0.095 MPa for 20 min reduces air entrainment before the impregnation bath is held at 32°C. At this temperature the formulated resin viscosity remains between 1,800 mPa·s and 2,500 mPa·s. Winding tension for 12K carbon roving is limited to 10–15 N per roving to prevent fibre compaction beyond 55% fibre volume fraction. The terminal finished product is a Type IV CNG or hydrogen storage vessel with a thermoplastic liner overwrapped by carbon-reinforced epoxy.

    The cure schedule for a 30 mm wall thickness is 80°C for 2 h, ramp at 1.5 K/min to 120°C for 2 h, then ramp at 1.0 K/min to 140°C for 3 h. Ramping above 2.0 K/min through the 100–120°C window produces a residual cure exotherm that exceeds the glass transition of the partially cured matrix, generating microvoids at the liner interface. Finished vessels are subjected to hydrostatic burst testing per ISO 11439:2013. Published data for CSN-010-specific liner compatibility in hydrogen service is limited; qualification batches must include cyclic hydraulic testing because the anhydride-cured network is susceptible to stress relaxation when exposed to sustained load above 60°C.

    Why Does Filler Loading Above 170 phr Shift the Breakdown Strength of CSN-010 Castings?

    Increasing fused silica addition from 100 phr to 200 phr reduces the coefficient of linear thermal expansion from approximately 41×10−6 K−1 to 25×10−6 K−1, but the same gradient raises mixed viscosity from 48,000 mPa·s to 240,000 mPa·s at 25°C. The change in dielectric breakdown strength is controlled by void content and filler wetting, not by resin polarity alone.

    Fused silica loading (phr)Mixed viscosity at 25°C (mPa·s)CTE (10⁻⁶ K⁻¹)Thermal conductivity (W/m·K)UL 94 vertical burn at 3 mmDielectric breakdown strength (kV/mm)
    012,500680.18HB16
    10048,000410.42HB19
    170127,000290.67V-020
    200240,000250.79V-021

    At filler loading above 170 phr, wetting time in a 200 L planetary mixer increases from 40 min to 90 min under −0.09 MPa absolute pressure. In production potting lines the encapsulant is preheated to 45°C before dispensing through static mixers with 24 elements. Cured castings at 170 phr fused silica attain a glass transition temperature of 138°C after 2 h at 100°C and 4 h at 150°C. Volume resistivity after 168 h at 85% RH and 85°C remains above 1×1013 Ω·m when tested according to ASTM D257-14. The limiting operational boundary is the exotherm at cast cross-sections above 25 mm; a gel time below 45 min at 80°C triggers thermal run-away in the centre of the mass. Filler loading is therefore capped at 200 phr for thick-section electronic encapsulations despite further CTE reduction available at 250 phr.

    At 5°C steel surface temperature, a phenalkamine-cured CSN-010 primer maintains wetting only when the epoxy-to-amine hydrogen equivalent ratio is held between 0.88:1.0 and 0.92:1.0. Outside this window, the film exhibits amine blush or incomplete through-cure. The coating is formulated as a high-solids marine primer at 82–85% volume solids, using 100 phr CSN-010, 55 phr phenalkamine hardener, 20 phr iron oxide, 10 phr talc, and 5 phr benzyl alcohol as de-aeration aid. Steel must be abrasive blast-cleaned to ISO 8501-1:2007 Sa 2½, and soluble chloride contamination should remain below 50 mg/m² by ISO 8502-6.

    Application is performed with airless spray equipment at 150 bar fluid pressure, using a 0.019 inch tungsten carbide tip. The specified dry film thickness is 200 µm, applied in two passes. The terminal finished product is a corrosion-resistant primer for ballast tanks, offshore structures, and coastal steelwork. After 2,000 h neutral salt spray per ASTM B117, scribe creep on panels coated with a compatible epoxy topcoat remains below 2.0 mm. Pull-off adhesion by ISO 4624 exceeds 5 MPa on dry blasted steel. Do not substitute a standard polyamide hardener for cure below 10°C; the phenalkamine chemistry is required to maintain film formation and through-cure at low temperature.

    When Post-Cure Oven Ramp Exceeds 3 K/min in Thick-Section Adhesive Bonds

    Structural paste adhesives based on CSN-010 are prepared by pre-dispersion of 12 phr of a carboxyl-terminated butadiene-acrylonitrile elastomer. The addition of 4 phr hydrophobic fumed silica controls slump on vertical automotive aluminium substrates. In a bond line of 3 mm thickness, oven ramp rates above 3 K/min generate a thermal gradient between the substrate and the bond centre. The resulting internal stress reduces lap shear strength by more than 15% when tested after 7 days at 23°C according to ASTM D1002-10.

    The preferred cure is 60 min at 80°C followed by 30 min at 120°C. Bulk mixed adhesive has a pot life of 55 min at 23°C, measured as the time for mixed viscosity to double from 180,000 mPa·s. Application through a meter-mix unit fitted with a 12-element static mixer produces a bead with a maximum width of 3 mm. Bonding aluminium alloy 5754 requires degreasing and phosphoric acid anodizing. After 1,000 h of neutral salt spray per ISO 9227:2017, average lap shear retention is 78% relative to dry controls. Formulators should avoid addition of unmodified polyamide hardener above 40 phr because network plasticization reduces glass transition temperature below 60°C and compromises creep resistance at 80°C.

    B-Stage Resin Flow Control for Lead-Free PCB Laminate Press Cycles

    For glass fabric style 7628 with a silane finish, CSN-010 is varnished at 55–60% solids in methyl ethyl ketone and advanced with dicyandiamide at 3.0 phr plus 2-methylimidazole at 0.08 phr. The varnisher line speed is set to yield a dry prepreg resin content of 40–45% and a B-stage resin flow of 25–35% by IPC-TM-650 method 2.3.17.2 at 170°C. Flow below 22% produces dry fibre regions at the laminate surface; flow above 38% causes resin starvation at the pattern edge and loss of copper peel strength.

    The press cycle uses 2.5 MPa specific pressure and a 190°C cure for 90 min. The fully cured laminate attains a glass transition temperature above 150°C by dynamic mechanical analysis, which is required for the 288°C solder float test described in IPC-TM-650 method 2.4.13.1. Z-axis thermal expansion from 50°C to 260°C should remain below 70×10−6 K−1. The laminate is classified under IPC-4101C/21 and must achieve UL 94 V-0 at 0.8 mm thickness. Where CSN-010-specific data for dicyandiamide advancement is limited, batch qualification is performed by measuring gel time at 170°C and comparing against a reference resin of equivalent epoxy equivalent weight rather than relying on supplier nominal values only.

    Aggregate-Bridged Crack Propagation in Epoxy Polymer Concrete Overlays

    Oven-dried silica sand and 2–5 mm basalt aggregate are mixed with CSN-010 at a resin-to-aggregate ratio of 1:10 by weight. The aggregate must contain less than 0.1 wt% free moisture before mixing to prevent amine-carbamate formation at the aggregate interface when a cycloaliphatic amine hardener is used. A forced-action pan mixer of 500 L capacity provides the required high-shear dispersion without generating aggregate fracture. The mixed material is placed in 40 mm lifts and consolidated with a needle vibrator.

    Compressive strength specimens are cured for 7 days at 23°C and tested per ASTM C579-18. Typical 7-day values are 80–90 MPa compressive and 20–25 MPa flexural. The low coefficient of thermal expansion of the resin phase is critical where steel anchor plates are cast in place; thermal cycling between −20°C and 60°C produces less than 0.2 mm crack opening at the resin–aggregate interface. Installation is not recommended below 10°C because the mixed viscosity exceeds 20,000 mPa·s and entrapped air cannot escape before gel. For machine base grouting, the maximum pour depth per lift is 50 mm; greater depths require cooled aggregate or a post-cure step to limit residual shrinkage.

    For vacuum-infused carbon composite skin panels, CSN-010 is blended with 10–15 phr of 1,4-butanediol diglycidyl ether to reduce initial viscosity to below 500 mPa·s at 30°C. The pot life at 30°C is extended to 3 h by selecting isophoronediamine as the hardener and holding the infusion catch-pot temperature at 25°C. The dry preform is assembled from 400 g/m² unidirectional carbon non-crimp fabric in a four-layer stack and compacted under −0.1 MPa vacuum. Resin inlet is positioned at the centre of the panel and the outlet at the perimeter to maintain a differential pressure of 0.02 MPa during infusion.

    The infused panel is cured for 2 h at 80°C and 2 h at 120°C. Void content is kept below 1% when measured by ASTM D2734-16, and the cured laminate achieves a dry glass transition temperature above 105°C. If relative humidity exceeds 60% during fabric lay-up, pre-drying at 60°C for 2 h is mandatory because moisture adsorbed on carbon fabric catalyses carbamate formation with isophoronediamine, lowering glass transition temperature by 10–15 K. The terminal finished product is a lightweight structural sandwich panel for marine or industrial enclosures.

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    Certification & Compliance
    More Introduction

    CSN-010 is identified as a liquid epoxy resin based on bisphenol-A diglycidyl ether chemistry. The model designation is a product identifier rather than a fixed statement of molecular specification; batch-specific epoxy equivalent weight, viscosity at 25 °C, hydrolyzable chloride content, and residual volatile content are controlled by the supplier’s certificate of analysis and should not be inferred from typical values assigned to other bisphenol-A diglycidyl ether liquids. Published data for this exact configuration is limited; therefore, process design must begin with the product data sheet and a pre-screen using the relevant ISO/ASTM methods listed below.

    Property or responseStandard test methodRelevance to CSN-010 processing
    Epoxy equivalent weightASTM D1652-11, ISO 3001:1999Stoichiometric hardener demand for amine or anhydride cure
    Viscosity at 25 °CISO 3219:1993, ASTM D2196-20Meter-mix pump sizing, wetting speed, and filler loading
    Hydrolyzable chloride contentASTM D1726-11, ISO 21627-3Corrosion risk in electronic and metal-bonded assemblies
    Platinum-cobalt colourISO 6271:2015, ASTM D1209-05Optical clarity and yellowing potential in clear coats
    Water absorption after cureISO 62:2008Property retention under humid service and thermal shock
    Tensile properties of cast neat resinASTM D638-14, ISO 527-2:2012Baseline strength and modulus before filler or plasticizer addition
    Glass transition temperatureISO 11357-2:2020Upper service temperature and post-cure completion
    Dielectric strengthASTM D149-20, IEC 60243-1:2013Electrical insulation and potting

    What Determines the Handling Window for CSN-010 During Metered Mixing?

    For liquid epoxy resins in the CSN-010 molecular-weight class, viscosity at 25 °C is typically high enough to require heated metering when dense fillers or long static-mixer paths are used. Low-molecular-weight unmodified bisphenol-A diglycidyl ether resins commonly exhibit a viscosity band of 9–16 Pa·s; the CSN-010 batch value must be verified because a deviation of 2 Pa·s at ambient temperature can shift pump back-pressure and alter mixing quality in positive-displacement two-component equipment. Preheating to 30–40 °C reduces viscosity but also accelerates the amine-epoxide reaction; the resulting pot life is commonly measured as the time to reach 10× the initial viscosity under isothermal conditions. The resin should not be stored in open containers at relative humidity above 60% because water uptake can promote amine blush and surface tack after cure. Avoid blending with amine-based additives prior to proper formulation review because premature exotherm and local gelation may occur. The processing window is bounded by pump inlet pressure, static-mixer pressure drop, and the onset of viscosity rise after curative injection. Rotational viscosity is measured according to ISO 3219:1993, while cure kinetics can be tracked by differential scanning calorimetry under ISO 11357-5:2013.

    CSN-010-derived cured networks are evaluated for immersion service using the mass, dimensional, and hardness change procedures of ASTM D543-14 or ISO 2812-1:2017. In an aromatic bisphenol-A backbone, the cured network typically exhibits greater resistance to aliphatic hydrocarbons and dilute alkali than a cycloaliphatic system of comparable crosslink density, but lower resistance to strong oxidizing acids and to solvents that swell the cured matrix. Solvent resistance is frequently monitored by methyl ethyl ketone double rubs under ASTM D5402-19; the result is not a bulk chemical resistance test but provides a rapid relative indication of crosslink density. For tank linings, the system must be tested in the actual chemical mixture at the service temperature because minor contaminants such as chlorinated solvents or free phenol can alter attack mechanisms. Humidity exposure during cure can produce amine blush on unmodified amine-cured surfaces; therefore, the working environment must be controlled below 60% RH or the formulation must include blush-resistant hardeners.

    Electrical Encapsulation Under Thermal Cycling and Partial Discharge Stress

    In potting and encapsulation, the critical parameters are dielectric strength, glass transition temperature, and thermal expansion. Dielectric breakdown is tested according to ASTM D149-20 or IEC 60243-1:2013; values for neat bisphenol-A networks are not a direct predictor of the filled system, because silica or calcium carbonate fillers change permittivity and internal stress distribution. The glass transition temperature after post-cure is measured by ISO 11357-2:2020. Thermal shock testing, commonly between -40 °C and 125 °C, is used to assess crack resistance around embedded metallic inserts. Unmodified aromatic epoxy systems of this class can develop higher shrinkage and internal stress than flexible polyurethane or silicone systems; therefore, designs with large copper busbars or sharp insert geometries require low exotherm cure and appropriate filler loading. Cycloaliphatic epoxy resins differ by offering lower viscosity before cure and better resistance to carbon tracking under electrical stress, but they usually require anhydride cure and high-temperature cure schedules. Published data for the CSN-010 electrical performance across all filler systems is limited, and electrical qualification must be performed on the final assembly.

    In structural grouting and concrete repair, CSN-010 can be formulated with clean dried aggregates to produce a moisture-insensitive epoxy binder when cured with amidoamine or cycloaliphatic amine systems. The relevant classification for epoxy bonding adhesives used in concrete is ASTM C881/C881M-20a, which assigns type, grade, and class based on application temperature and viscosity. A low-molecular-weight liquid bisphenol-A diglycidyl ether resin is often selected over a solid high-molecular-weight epoxy because the liquid form permits ambient mixing without solvent; however, the higher exotherm of low-molecular-weight resins limits the maximum neat thickness. The compressive strength of an epoxy concrete or mortar is measured according to ASTM C579-18, while bond strength to concrete is evaluated by pull-off testing, commonly in accordance with ASTM D4541-17. Aggregates and fillers should be pre-dried at 110 °C to constant mass when ambient relative humidity exceeds 60%. The cure rate slows sharply below 10 °C; hardener selection must therefore match the substrate temperature rather than the air temperature.

    When the Resin Is Evaluated for Vacuum-Assisted Wet Lay-Up, Viscosity Reduction Becomes the Governing Constraint

    Unmodified epoxy resins of the CSN-010 molecular-weight range are generally too viscous for reliable vacuum bag infusion at ambient temperature unless heated to 50–60 °C or blended with a reactive diluent. Infusion resins are commonly specified below 1000 mPa·s at the bag entry temperature; a neat viscosity above 1 Pa·s may cause slow pleat filling and locally dry fiber. Heating reduces viscosity but also reduces pot life and can create uneven cure if the mould heat is not uniform. Reactive diluents such as 1,4-butanediol diglycidyl ether lower viscosity and improve wetting, but each 10 phr addition can reduce crosslink density and chemically shift the cured network; the glass transition temperature and solvent resistance must be rechecked against ISO 11357-2:2020 and ASTM D5402-19. In contrast, solid high-molecular-weight epoxy resins cannot be processed by this route without solvent or high-temperature application. The vacuum infusion process must account for volatile stripping of residual epichlorohydrin; vacuum level and resin temperature should be validated in a full-scale dry run.

    Acid Service Versus Novolac and Cycloaliphatic Backbones

    The aromatic rings and ether linkages in bisphenol-A based CSN-010 provide a specific resistance profile that differs from epoxidized novolac and cycloaliphatic resins. Epoxidized novolac resins generally have a higher functionality per molecule, producing greater crosslink density after cure and improved retained strength in hot sulfuric acid or mixed solvent streams; correspondingly, they often exhibit higher viscosity and require higher processing temperatures. Cycloaliphatic epoxy resins resist ultraviolet yellowing and electrical carbon tracking better than bisphenol-A systems, but their resistance to some organic acids and their compatibility with amine curatives are lower; anhydride cure is commonly required. In sulfuric acid at 50 °C, an unmodified bisphenol-A network may show measurable mass loss as the ether linkages are attacked, while a novolac-cured system may retain integrity longer. The comparison is not absolute; for any CSN-010 formulation, long-term immersion must be tested under ASTM D543-14 or ISO 2812-1:2017 using the actual service concentration and temperature. Silica-filled CSN-010 is preferred over unfilled resin when acid permeability and thermal expansion must be reduced.

    CSN-010 can be formulated into self-leveling floor systems and trowel-applied mortars. Flow, surface appearance, and air release are controlled by viscosity and filler morphology; working time is determined by gel-time measurement and by viscosity build to a specified upper limit. Adhesion to concrete is assessed by ASTM D4541-17, and surface hardness is measured as Shore D under ASTM D2240-15 or ISO 868:2003. Aromatic bisphenol-A resins such as CSN-010 generally have lower ultraviolet stability than aliphatic or cycloaliphatic systems and will amber if left unpigmented in direct sunlight. Therefore, unpigmented systems exposed to sunlight should be topcoated with an aliphatic urethane or an acrylic. Avoid application when substrate temperature is below 10 °C or when the substrate is less than 3 °C above the dew point, because condensation disrupts adhesion and can produce microscopic voids.

    How Does the CSN-010 Cured Network Respond to Long-Term Humid Ageing?

    Water absorption in cured bisphenol-A networks is commonly measured under ISO 62:2008; immersion at 60 °C accelerates saturation and reveals whether glass transition temperature depression is reversible or irreversible. Absorbed water can plasticize the matrix, reducing tensile modulus and increasing dielectric loss factor. Dielectric constant and dissipation factor are measured according to ASTM D150-18. For long-term humid ageing, property retention is benchmarked against ISO 175:2010 for plastics in contact with liquids. The CSN-010 system should be subjected to humidity preconditioning before electrical or mechanical testing because moisture from ambient storage can mask true dry network properties. Aromatic bisphenol-A networks are generally more susceptible to moisture plasticization than cycloaliphatic systems of equivalent crosslink density when cured with amine hardeners; anhydride-cured systems may show lower water uptake but require accurate accelerator ratios and are sensitive to incomplete post-cure. Data for this specific configuration under condensing humidity cycles is limited; the user must generate lot-specific ageing curves.

    In castings greater than 25 mm in neat thickness, the rate of heat generation from the amine-epoxide reaction can exceed the rate of heat transfer to the mould, resulting in a bulk temperature overshoot that discolors the resin, lowers viscosity prematurely, and may induce cracking during cool-down. The maximum safe pour thickness is determined by cure exotherm, mould material, and surrounding temperature; low-molecular-weight bisphenol-A resins release more heat per unit mass than higher-molecular-weight solid resins and usually cannot be cast as 50 mm clear blocks without staged cure or fillers. Temperature rise may be tracked by inserting thermocouples at the core and monitoring against a predetermined limit, such as 80 °C for clear castings. Fillers with high thermal conductivity, such as aluminum oxide, reduce peak exotherm and lower residual internal stress. This thermal boundary is a practical difference from flexible silicone or polyurethane casting resins; those systems can be cast thicker because their lower reaction exotherm or lower modulus dissipates stress differently, but they do not provide the same compressive stiffness or chemical resistance as an epoxy network. The operational limit must be validated on production-scale moulds because laboratory-scale exotherm measurements do not capture the heat loss conditions of large production tools.